error
Divisa

GC-MS OF BIOLOGICALLY AND ENVIRONMENTALLY SIGNIFICANT ORGANIC COMPOUNDS

TMS DERIVATIVES

9781119611349 ::  GC-MS OF BIOLOGICALLY AND ENVIRONMENTALLY SIGNIFICANT ORGANIC COMPOUNDS
ISBN:

9781119611349

EditorialJOHN WILEY & SONS LTD.
Edició:
Pàgines:720
Idioma:INGLES
P.V.P.: 466,54 € + 4% IVA = 485,20 €
Dto 5% Estalvies 24,26 €
Import final iva incl. 460,94 €
EN STOCK / ENVIAMENT EN 8-10 DIAS

PREFACE VII1 INTRODUCTION 12 GAS CHROMATOGRAPHY AND MASS SPECTROMETRY CONSIDERATIONS 72.1 SILYLATION REAGENTS AND PROCEDURE OF DERIVATISATION 72.2 TWO-STEP DERIVATISATION: OXIMATING SILYLATING 82.3 ANALYTICAL PROCEDURE 102.3.1 SELECTION OF STATIONARY PHASE AND CONDITIONS OF SEPARATION 102.3.2 SAMPLE PREPARATION 102.3.3 QUALITATIVE MS IDENTIFICATION 122.3.3.1 ALIPHATIC ALCOHOLS 162.3.3.2 AROMATIC ALCOHOLS 162.3.3.3 CARBOXYLIC ACIDS 162.3.3.4 AMINO ACIDS 162.3.3.5 PHENYLPROPANOIDS 172.3.3.6 FLAVONOIDS 182.3.3.7 STEROIDS 202.3.3.8 CARBOHYDRATES AND GLYCOSIDES 222.4 A CRITICAL ROLE OF RETENTION INDICES IN GS-MS INVESTIGATIONS 242.5 EXPERIMENTAL FACTORS INFLUENCING THE ACCURACY OF RETENTION INDICES 282.6 POSSIBLE ARTEFACTS AND COMPLICATIONS OF MASS SPECTRAL IDENTIFICATION 303 EXPLANATION OF FORMAT USED IN THE BOOK 334 REFERENCES 355 ALPHABETIC LISTING OF COMPOUNDS 436 COMPOUNDS LISTED IN ORDER OF THEIR RETENTION INDICES 877 MASS SPECTRA AND RETENTION INDICES OF TMS DERIVATIVES 131

PROVIDES A COMPREHENSIVE GUIDE TO THE USE OF GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ON ENVIRONMENTALLY SIGNIFICANT ORGANIC COMPOUNDS THIS BOOK PRESENTS A LIBRARY OF MASS SPECTRA OF 1,725 BIOLOGICALLY AND ENVIRONMENTALLY IMPORTANT ORGANIC COMPOUNDS, IN THE FORM OF THEIR TRIMETHYLSILYL DERIVATIVES (TMS), AS WELL AS THEIR LINEAR TEMPERATURE PROGRAMMED CHROMATOGRAPHIC RETENTION INDICES, RI, WHOSE VALUES ARE IN THE RANGE OF 700-4700 INDEX UNITS. OF THE COMPOUNDS PRESENTED, MORE THAN 60% OF COMPOUNDS HAVE NOT PREVIOUSLY BEEN CHARACTERIZED BY THEIR MASS SPECTRA, AND MORE THAN 70% NOT PREVIOUSLY BEEN CHARACTERIZED BY THEIR RI VALUES. SOME OF THESE COMPOUNDS, NEVER BEFORE ANALYSED VIA MS AND GC, WERE DETECTED BY THE AUTHOR'S TEAM IN PLANT TISSUES. THE FIRST CHAPTERS OF THE BOOK ARE DEVOTED TO THE METHODOLOGY AND PRACTICE OF SAMPLE PREPARATION, AS WELL AS TO MASS SPECTROMETRY CONSIDERATIONS. THEY CONTAIN THE DISCUSSION OF POSSIBLE COMPLICATIONS AND LIMITATIONS OF THE METHOD. THE BOOK INCLUDES LISTS OF CHEMICAL COMPOUNDS IN ALPHABETICAL ORDER, AS WELL AS IN THE ORDER OF THEIR RETENTION INDICES WHICH FACILITATES THE SEARCH FOR PARAMETERS OF INTEREST. EVERY COMPOUND IN THE BOOK INCLUDES A RI VALUE, MASS SPECTRUM, CAS NUMBER (IF AVAILABLE), MOLECULAR AND STRUCTURAL FORMULA, FORMULA WEIGHT, CHEMICAL NAME AND LIST OF SYNONYMS, AS WELL THE SOURCE OF COMPOUNDS USED FOR REGISTRATION OF SPECTRUM AND RI VALUE. FEATURES MASS SPECTRA AND CHROMATOGRAPHIC RETENTION INDICES OF 1,725 ORGANIC SUBSTANCES IN THE FORM OF THEIR TRIMETHYLSILYL DERIVATIVES (TMS)INCLUDES THE CAS NUMBER, MOLECULAR AND STRUCTURAL FORMULA, FORMULA WEIGHT, MASS SPECTRUM, CHEMICAL NAME AND LIST OF SYNONYMS, AND MORE FOR EVERY COMPOUND COVERED WITHINTHE FIRST PUBLICATION CONTAINING ANALYTICAL PARAMETERS OF HIGH-BOILING COMPOUNDS SUCH AS GLYCOSIDES, LIGNANS, AND PHENYLPROPENOID GLYCERIDES WITH RI VALUES >4000 GC-MS OF BIOLOGICALLY AND ENVIRONMENTALLY SIGNIFICANT ORGANIC COMPOUNDS WILL APPEAL TO SPECIALISTS IN PHYTOCHEMICAL ANALYSIS, FOOD, AND ENVIRONMENTAL CHEMISTRY, AS WELL AS OTHER INVESTIGATORS DEALING WITH GC OR GC/MS ANALYSIS COMPLEX MIXTURES OF ORGANIC COMPOUNDS.

THE ACCOMPANYING ELECTRONIC DATABASE, "BIOLOGICALLY AND ENVIRONMENTALLY IMPORTANT ORGANIC COMPOUNDS - GCMS LIBRARY", WILL BE PUBLISHED IN MID-2020, ISBN: 978-1-119-60170-8.





QUIMICA
Llibres relacionats
ISBN: 9780128189658 INORGANIC POLLUTANTS IN WATERINORGANIC POLLUTANTS IN WATER
9780128189658
Marzo 2020

113€ S/I
107,35€ S/I

ISBN: 9780471659372 1HNMR OF ORGANIC COMPOUNDS, VOLUME 31HNMR OF ORGANIC COMPOUNDS, VOLUME 3
9780471659372
Abril 2020

4.393,69€ S/I

ISBN: 9781118887813 MACROMOLECULAR SELF-ASSEMBLYMACROMOLECULAR SELF-ASSEMBLY
9781118887813
Abril 2020

118.11€ S/I
112,20€ S/I

ISBN: 9781118939314 APPLICATION OF NANOTECHNOLOGY IN WATER RESEARCHAPPLICATION OF NANOTECHNOLOGY IN WATER ...
9781118939314
Abril 2020

153.54€ S/I
145,86€ S/I

ISBN: 9781119251101 MULTIPHASE REACTOR ENGINEERING FOR CLEAN AND LOW-CARBON ENERGY APPLICATIONSMULTIPHASE REACTOR ENGINEERING FOR ...
9781119251101
Abril 2020

184.25€ S/I
175,04€ S/I